HCID 59054439, compound → HCID 59053463, compound
Reaction equation
[Cl:1][C:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]=[CH:4][C:3]=1[S:12]([CH2:15][CH2:16][NH:17][CH2:18][C:19]1O[CH:21]=[CH:22][CH:23]=1)(=[O:14])=[O:13].ClC1C2C(=CC=CC=2)C=CC=1SC[CH2:37][NH:38]CC1C=CC=CN=1>>[Cl:1][C:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]=[CH:4][C:3]=1[S:12]([CH2:15][CH2:16][NH:17][CH2:18][C:19]1[CH:23]=[CH:22][CH:21]=[CH:37][N:38]=1)(=[O:14])=[O:13]Participants
3
Procedure
Prepared as described for compound 25 from 2-[(1-chloronaphthalen-2-yl)sulfanyl]-N-(pyridin-2-ylmethyl)ethanamine in 78% yield as yellow oil.
Workup
- customPrepared
Sources & evidence
- ORD record
- ord-87193d08dc7e4c859ca62b7cf6242e70
- Source dataset
- uspto-grants-2014_12
- Patent number
- US08906946B2
Reaction notes
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