Methyl iodide → HCID 59053529, compound

Participants

Reaction Steps

A solution of 2-[(1-chloronaphthalen-2-yl)oxy]-N-(furan-2-ylmethyl)-N-methylethanamine (38) (0.05 mmol) was dissolved in 3 mL of THF; then 0.10 mmol of MeI were added under stirring and allowed to react for 14 h at room temperature. The solvent was evaporated under vacuum and the resulting crude was triturated with 5 mL of n-hexane for 2 h. The solid was filtered and dried at 50° C. under reduce pressure to afford 2-[(1-chloronaphthalen-2-yl)oxy]-N-(furan-2-ylmethyl)-N,N-dimethylethanaminium iodide as a white solid (92% yield).

Provenance & Evidence