5-Chloro-2-furaldehyde → HCID 59053534, compound

HRID 1400287Notes

Reaction equation

HRID 1400287 reaction equation
[Cl-].[Cl:2][C:3]1[C:12]2[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=2)[CH:6]=[CH:5][C:4]=1[NH:13][CH2:14][CH2:15][NH3+:16].[Cl:17][C:18]1[O:22][C:21]([CH:23]=O)=[CH:20][CH:19]=1>>[Cl:17][C:18]1[O:22][C:21]([CH2:23][NH:16][CH2:15][CH2:14][NH:13][C:4]2[CH:5]=[CH:6][C:7]3[C:12](=[CH:11][CH:10]=[CH:9][CH:8]=3)[C:3]=2[Cl:2])=[CH:20][CH:19]=1

Participants

3

Procedure

Prepared from 2-[(1-chloronaphthalen-2-yl)amino]ethanaminium chloride and 5-chlorofuran-2-carbaldehyde in 67% yield as a yellow oil.

Sources & evidence

ORD record
ord-5b8758fd96dd477a8ab23b551c0e1f69
Source dataset
uspto-grants-2014_12
Patent number
US08906946B2

Reaction notes

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