1,1'-Carbonyldiimidazole → HCID 58474481, compound

Participants

Reaction Steps

To a solution of 196 (0.9 g, 3.67 mmol) in DCM (30 mL) was added CDI (0.595 g, 3.67 mmol), and the reaction mixture was stirred at RT over weekend. The mixture was then concentrated and the residue was purified by flash column chromatography (eluent EtOAc) to afford the title compound 197 (373 mg, 38% yield) as colorless oil. MS: 271 (HM+).

Provenance & Evidence