Acrylate → Cyclohexene, 1-((trimethylsilyl)oxy)-

Participants

Reaction Conditions

Reaction Steps

In a pressure vessel, a solution of acrylate (1 eq), (buta-1,3-dien-2-yloxy)trimethylsilane (1.1 eq) in toluene was flushed with nitrogen, sealed and heated at 150° C. for 1-3 days. The reaction mixture was cooled to RT and concentrated in vacuo to give crude product which was used for the next step without purification.

Provenance & Evidence