Methyl iodide → HCID 117722888, compound

HRID 1401359Notes

Reaction equation

HRID 1401359 reaction equation
[C:1]1([N:7]2[CH:11]=[C:10]([CH:12]=[CH2:13])[N:9]=[N:8]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[I:14][CH3:15]>O>[I-:14].[CH3:15][N+:9]1[C:10]([CH:12]=[CH2:13])=[CH:11][N:7]([C:1]2[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=2)[N:8]=1

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 53473125HCID 53473125, compound

Product 1

HCID 117722888HCID 117722888, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

1-phenyl-4-vinyl-1H-1,2,3-triazole (0.9 g, 5.26 mmol) and iodomethane (37.3 g, 263 mmol) were mixed and stirred overnight. Water was added and the salt was extracted in water. The water was removed under vacuum and the precipitate was washed with acetone and the acetone was decanted yielding pale yellow crystals.

Workup

  1. extractionthe salt was extracted in water
  2. customThe water was removed under vacuum
  3. washthe precipitate was washed with acetone
  4. customthe acetone was decanted
  5. customyielding pale yellow crystals

Sources & evidence

ORD record
ord-7a4b5742604e41ec933b26908c0dc756
Source dataset
uspto-grants-2014_12
Patent number
US08907105B1

Reaction notes

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