Methyl iodide → HCID 178444668, compound

HRID 1401362Notes

Reaction equation

HRID 1401362 reaction equation
[CH2:1]([N:7]1[CH:11]=[C:10]([C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)[N:9]=[N:8]1)[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6].[I:18][CH3:19]>>[I-:18].[CH2:1]([N:7]1[CH:11]=[C:10]([C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)[N+:9]([CH3:19])=[N:8]1)[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6]

Participants

3

Reactant 2

HCID 6328Methyl iodide2×HCID 67199508HCID 67199508, compound

Product 1

HCID 178444668HCID 178444668, compound

Conditions

Temperature
40 °C

Procedure

1-hexyl-4-phenyl-1H-1,2,3-triazole (0.58 g, 2.53 mmol) and iodomethane (2 ml, 32.0 mmol) were added to a 20 mL vial. The reaction was heated at 40° C. for 3 days. The iodomethane was allowed to evaporate in the hood. The following structure was confirmed:

Workup

  1. customto evaporate in the hood

Sources & evidence

ORD record
ord-c686a3ff81374b27aaa80d12bb242e83
Source dataset
uspto-grants-2014_12
Patent number
US08907105B1

Reaction notes

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