Methyl iodide → HCID 178442419, compound

HRID 1401365Notes

Reaction equation

HRID 1401365 reaction equation
[CH2:1]([C:7]1[N:8]=[N:9][N:10]([CH2:12][CH2:13][CH3:14])[CH:11]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6].[I:15][CH3:16]>>[I-:15].[CH2:1]([C:7]1[N+:8]([CH3:16])=[N:9][N:10]([CH2:12][CH2:13][CH3:14])[CH:11]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6]

Participants

3

Reactant 2

HCID 6328Methyl iodide2×HCID 68301825HCID 68301825, compound

Product 1

HCID 178442419HCID 178442419, compound

Conditions

Temperature
40 °C

Procedure

4-hexyl-1-propyl-1H-1,2,3-triazole and excess iodomethane were added to a 20 mL vial. The reaction was heated at 40° C. for 3 days. The iodomethane was allowed to evaporate in the hood. The following structure of 4-hexyl-3-methyl-1-propyl-1H-1,2,3-triazol-3-ium iodide was confirmed:

Workup

  1. customto evaporate in the hood

Sources & evidence

ORD record
ord-855e4e60ba6f455390c39d4e6c637b6a
Source dataset
uspto-grants-2014_12
Patent number
US08907105B1

Reaction notes

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