反应详情

1-propyl-4-((trimethylsilyl)methyl)-1H-1,2,3-triazole and excess iodomethane were added to a vial. The reaction was heated for 19.5 hours and 5 mL ACN was added. The reaction was heated for another 2 hours. The precipitate was filtered, rinsed with ether and dried in vacuo overnight. The following 3-methyl-1-propyl-4-((trimethylsilyl)methyl)-1H-1,2,3-triazol-3-ium iodide structure was confirmed:

1. temperatureThe reaction was heated for 19.5 hours
2. temperatureThe reaction was heated for another 2 hours
3. filtrationThe precipitate was filtered
4. washrinsed with ether
5. customdried in vacuo overnight