p-(Octyloxy)benzaldehyde → HCID 89500558, compound

HRID 1401725Notes

Reaction equation

[CH3:1][C:2]1[CH:7]=[CH:6][C:5]2[O:8][CH2:9][C:10]([CH2:12][O:13][C:4]=2[CH:3]=1)=[O:11].[CH2:14]([O:22][C:23]1[CH:30]=[CH:29][C:26]([CH:27]=O)=[CH:25][CH:24]=1)[CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH3:21]>>[CH3:1][C:2]1[CH:7]=[CH:6][C:5]2[O:8]/[C:9](=[CH:27]\[C:26]3[CH:29]=[CH:30][C:23]([O:22][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH3:21])=[CH:24][CH:25]=3)/[C:10](=[O:11])/[C:12](=[CH:27]/[C:26]3[CH:29]=[CH:30][C:23]([O:22][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH3:21])=[CH:24][CH:25]=3)/[O:13][C:4]=2[CH:3]=1

Participants

Reactant 2

HCID 90358p-(Octyloxy)benzaldehyde

HCID 120101Methyl benzodioxepinone

Product 1

HCID 89500558HCID 89500558, compound

Procedure

Calone is reacted with 4-octyloxybenzaldehyde analogously to the reaction conditions of Example 1, giving 7-methyl-2,4-bis[1-(4-octyloxyphenyl)meth-(Z)-ylidene]benzo[b]-1,4-dioxepin-3-one.

Sources & evidence

ORD record: ord-6c41e469e547485b88b980febac24d7a
Source dataset: uspto-grants-2014_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08907110B2

Reaction notes

Loading…