HRID1401751

反应详情

EQUATION

反应方程式

HRID 1401751 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

The output from the aldolization comprising crude 2-propylheptenal was hydrogenated selectively in the liquid phase over the palladium catalyst H 14535 (0.5% of Pd on aluminium oxide), procured from Degussa, at 160° C. and 2.5 MPa in a circulation apparatus to form 2-propylheptanal. For this purpose, 200 ml/h of starting material were passed continuously over 400 ml of catalyst, corresponding to a space velocity over the catalyst of 0.5 h−1.

WORKUP

后处理

  1. customprocured from Degussa, at 160° C.