HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Hydroxypentanal → HCID 67324498, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Hydroxypentanal | HCID 20205 | — |
| Reactant | HCID 68381056 | HCID 68381056 | — |
| Product | HCID 67324498 | HCID 67324498 | — |
Reaction Steps
The preparation was carried out as already described via a reductive amination starting from 100 mg (0.28 mmol) of 4-[2-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalen-2-yl)thiazol-4-yl]piperidine hydrochloride (preparation already described above) and 58 mg (0.56 mmol) of 5-hydroxypentanal. The product was purified by means of preparative HPLC and is in the form of the hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08907098B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-833d4ffba30943cf9cb31d2d12f53a9b |
| Source note | uspto-grants-2014_12 |