HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Hydroxypentanal → HCID 67323350, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Hydroxypentanal | HCID 20205 | — |
| Reactant | HCID 53311789 | HCID 53311789 | — |
| Product | HCID 67323350 | HCID 67323350 | — |
Reaction Steps
The preparation was carried out as already described via a reductive amination starting from 125 mg (0.35 mmol) of 4-[5-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalen-2-yl)-1,3,4-thiadiazol-2-yl]piperidine and 72 mg (0.70 mmol) of 5-hydroxypentanal. The product was purified by means of preparative HPLC and converted into the hydrochloride by treatment with methanolic HCl.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08907098B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-89e7ed2085dd4352a9218985b379bb07 |
| Source note | uspto-grants-2014_12 |