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HRID1401830

反应详情

EQUATION

反应方程式

HRID 1401830 的结构方程式

REACTANTS

反应物

2
结构：CC1(C)CCC(C)(C)c2cc(C(=O)CBr)ccc21
HCID2801337

2-Bromo-1-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalen-2-yl)ethan-1-one

C16H21BrO

结构：NC(=S)N1CCC(O)CC1
HCID16790966

4-Hydroxy-1-piperidinecarbothioamide

C6H12N2OS

PRODUCTS

生成物

1
结构：CC1(C)CCC(C)(C)c2cc(-c3csc(N4CCC(O)CC4)n3)ccc21
HCID53311626

未命名化合物

PROCEDURE

实验过程

The preparation was carried out as already described starting from 397 mg (0.94 mmol) of 2-bromo-1-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalen-2-yl)ethanone and 100 mg (0.62 mmol) of 4-hydroxypiperidine-1-carbothioic acid amide from step a. The product was purified by means of preparative HPLC and is in the form of the hydrochloride.

WORKUP

后处理

  1. customThe product was purified by means of preparative HPLC