Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | HCID 89624295 | HCID 89624295 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 89612461 | HCID 89612461 | — |
Reaction Steps
To a solution of Intermediate 119f (0.10 mmol) in THF (2 mL) was added dimethylamine (2M in MeOH, 0.4 mL, 0.8 mmol) and the reaction stirred at 50° C. for 24 h. The crude reaction mixture was cooled and partitioned between EtOAc and water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08907094B2 |
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| Source dataset | uspto-grants-2014_12 |
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| ORD ID | ord-149a78ae15104fb883160cef366f2f73 |
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| Source note | uspto-grants-2014_12 |
|---|