Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1402364Generated: October 31, 2026

Dimethylamine → HCID 89612461, compound

https://huagongshe.com/reaction/1402364

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDimethylamineHCID 674—
ReactantHCID 89624295HCID 89624295—
SolventTetrahydrofuranHCID 8028—
ProductHCID 89612461HCID 89612461—

Reaction Conditions

Temperature50 °C

Reaction Steps

To a solution of Intermediate 119f (0.10 mmol) in THF (2 mL) was added dimethylamine (2M in MeOH, 0.4 mL, 0.8 mmol) and the reaction stirred at 50° C. for 24 h. The crude reaction mixture was cooled and partitioned between EtOAc and water.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08907094B2
Source datasetuspto-grants-2014_12
ORD IDord-149a78ae15104fb883160cef366f2f73
Source noteuspto-grants-2014_12