Diethyl Malonate → HCID 11669279, 화합물

HRID 1402850노트

반응식

[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([C:8](=[O:18])[CH:9]=[CH:10][C:11]2[CH:16]=[CH:15][C:14]([Cl:17])=[CH:13][CH:12]=2)=[CH:4][CH:3]=1.[C:19]([O:27][CH2:28][CH3:29])(=[O:26])[CH2:20][C:21]([O:23][CH2:24][CH3:25])=[O:22]>>[Cl:17][C:14]1[CH:13]=[CH:12][C:11]([CH:10]([CH:20]([C:21]([O:23][CH2:24][CH3:25])=[O:22])[C:19]([O:27][CH2:28][CH3:29])=[O:26])[CH2:9][C:8]([C:5]2[CH:6]=[CH:7][C:2]([Cl:1])=[CH:3][CH:4]=2)=[O:18])=[CH:16][CH:15]=1

참가 물질

반응물 2

HCID 7761Diethyl Malonate

HCID 2756324,4'-Dichloro chalcone

생성물 1

HCID 11669279HCID 11669279, 화합물

실험 절차

By a procedure similar to that of example 1.59.2, starting from 1,3-bis(4-chlorophenyl)-prop-2-en-1-one and diethyl malonate, diethyl 2-[1,3-bis(4-chlorophenyl)-3-oxopropyl]-malonate was obtained as colourless solid.

출처 및 근거

ORD 기록: ord-19d845fceb1f403a84c9fe9b494b2d40
출처 데이터셋: uspto-grants-2014_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08912186B2

반응 노트

불러오는 중…