2-Naphthalenecarboxaldehyde → HCID 66759886, compound
Reaction equation
[CH:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][C:2]=1[CH:11]=O.[CH3:13][C:14]([C:16]1[CH:21]=[CH:20][C:19]([I:22])=[CH:18][CH:17]=1)=[O:15]>>[I:22][C:19]1[CH:20]=[CH:21][C:16]([C:14](=[O:15])[CH:13]=[CH:11][C:2]2[CH:3]=[CH:4][C:5]3[C:10](=[CH:9][CH:8]=[CH:7][CH:6]=3)[CH:1]=2)=[CH:17][CH:18]=1Participants
3
Procedure
By a procedure similar to that of example 1.59.1, starting from 2-naphthaldehyde and 4-iodoacetophenone, 1-(4-iodophenyl)-3-(2-naphthalenyl)prop-2-en-1-one was obtained as yellowish solid.
Sources & evidence
- ORD record
- ord-233acc156ecc4e3080f160668c41579a
- Source dataset
- uspto-grants-2014_12
- Patent number
- US08912186B2
Reaction notes
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