Malononitrile → HCID 45381794, compound
Reaction equation
[I:1][C:2]1[CH:7]=[CH:6][C:5]([C:8](=[O:17])[CH:9]=[CH:10][C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)=[CH:4][CH:3]=1.[C:18](#[N:22])[CH2:19][C:20]#[N:21]>>[I:1][C:2]1[CH:3]=[CH:4][C:5]([C:8](=[O:17])[CH2:9][CH:10]([CH:19]([C:18]#[N:22])[C:20]#[N:21])[C:11]2[CH:12]=[CH:13][CH:14]=[CH:15][CH:16]=2)=[CH:6][CH:7]=1Participants
3
Procedure
By a procedure similar to that of example 1.59.2, starting from 1-(4-iodophenyl)-3-phenylprop-2-en-1-one and malononitrile, 2-(3-(4-iodophenyl)-3-oxo-1-phenylpropyl)malononitrile was obtained as colourless solid.
Sources & evidence
- ORD record
- ord-1579e54555fa455c9a0ac667ac3ecc21
- Source dataset
- uspto-grants-2014_12
- Patent number
- US08912186B2
Reaction notes
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