2-Naphthalenecarboxaldehyde → HCID 2794958, compound
Reaction equation
[CH:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][C:2]=1[CH:11]=[O:12].[CH:13]1[C:22]2[C:17](=[CH:18][CH:19]=[CH:20][CH:21]=2)[CH:16]=[CH:15][C:14]=1[C:23](=O)[CH3:24]>>[CH:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][C:2]=1[C:11](=[O:12])[CH:24]=[CH:23][C:14]1[CH:15]=[CH:16][C:17]2[C:22](=[CH:21][CH:20]=[CH:19][CH:18]=2)[CH:13]=1Participants
3
Procedure
Synthesised according to example 1.59.1, using 2-naphthaldehyde (10.9 g, 64.03 mmol) and 1-(naphthalen-2-yl)ethanone (11.9 g, 64.03 mmol); yellow solid; yield: 18.8 g (95%);
Workup
- customSynthesised
Sources & evidence
- ORD record
- ord-4e33aa27c50a4209879e5b7d60345008
- Source dataset
- uspto-grants-2014_12
- Patent number
- US08912186B2
Reaction notes
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