2-Acetylnaphthalene → HCID 66759032, compound

HRID 1402971Notes

Reaction equation

HRID 1402971 reaction equation
[CH3:1][O:2][CH2:3][O:4][C:5]1[CH:6]=[C:7]2[C:12](=[CH:13][CH:14]=1)[CH:11]=[C:10]([CH:15]=O)[CH:9]=[CH:8]2.[CH:17]1[C:26]2[C:21](=[CH:22][CH:23]=[CH:24][CH:25]=2)[CH:20]=[CH:19][C:18]=1[C:27](=[O:29])[CH3:28]>>[CH3:1][O:2][CH2:3][O:4][C:5]1[CH:6]=[C:7]2[C:12](=[CH:13][CH:14]=1)[CH:11]=[C:10]([CH:15]=[CH:28][C:27]([C:18]1[CH:19]=[CH:20][C:21]3[C:26](=[CH:25][CH:24]=[CH:23][CH:22]=3)[CH:17]=1)=[O:29])[CH:9]=[CH:8]2

Participants

3

Reactant 2

HCID 71222-AcetylnaphthaleneHCID 71533760HCID 71533760, compound

Product 1

HCID 66759032HCID 66759032, compound

Procedure

Synthesised according to example 1.59.1 using 6-(methoxymethoxy)-2-naphthaldehyde (2.0 g, 9.25 mmol) and 1-(naphthalen-2-yl)ethanone (1.57 g, 9.25 mmol); yellow solid; yield: 1.90 g (56%);

Workup

  1. customSynthesised

Sources & evidence

ORD record
ord-692e1532e74f443c9d829f19f2fcb5e3
Source dataset
uspto-grants-2014_12
Patent number
US08912186B2

Reaction notes

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