Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Benzyl-3-methyl-5-nitroindazole → 1-Benzyl-3-methyl-1H-indazol-5-ylamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Benzyl-3-methyl-5-nitroindazole | HCID 21952162 | — |
| 반응물 | HCID 178418361 | HCID 178418361 | — |
| 촉매 | Platinum | HCID 23939 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | 1-Benzyl-3-methyl-1H-indazol-5-ylamine | HCID 54103309 | — |
반응 단계
1-Benzyl-3-methyl-5-nitroindazole (0.15 g) in THF (15 ml) was treated with platinum on carbon (0.05 g, 5%) under an atmosphere of hydrogen at room temperature. When hydrogen uptake was complete, the mixture was filtered and concentrated in vacuo to give the title compound; m/z (M+1)+ 268.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08912205B2 |
| 출처 데이터셋 | uspto-grants-2014_12 |
| ORD ID | ord-2c1bb9d3b3044fc0b4ab44f0cdf7b342 |
| 출처 메모 | uspto-grants-2014_12 |