Aluminium lithium hydride → HCID 58303887, compound

Participants

Reaction Steps

To the solution of 9-4 (154 mg, 0.46 mmol) in anhydrous THF (10 mL) was added LiAlH4 (53 mg, 1.40 mmol). The mixture was heated to reflux for 2 h. Na2SO4.10H2O was added and the solid was filtered off. The filtrate was concentrated in vacuo to get a residue, which was purified by preparative TLC (DCM:MeOH:10:1) to afford compound 9-5 (30 mg, 27% yield) as white solid.

Provenance & Evidence