HCID 58303866, compound → HCID 50995814, compound

Participants

Reaction Steps

Following the procedure (step 6, scheme 17) used to prepare compound 17-7, compound 23-3 was used as starting material, giving compound 23-4 in 62% yield as a colorless oil, which was converted to the hydrochloride salt. 1H NMR (DMSO-d6, 300 MHz) δ (ppm) (HCl salt): 8.62 (br, 2H), 7.18-7.31 (m, 5H), 7.15 (s, 1H), 6.87 (d, J=13.4 Hz, 1H), 3.85 (d, J=1.7 Hz, 3H), 3.69 (s, 3H), 3.05-3.13 (m, 4H), 2.88 (br, 4H), 2.57 (s, 3H). LRMS: calc 340.2 found 341.1[MH]+.

Provenance & Evidence