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HRID1404908

反应详情

EQUATION

反应方程式

HRID 1404908 的结构方程式

REACTANTS

反应物

2
结构：Cc1cccc2c1N(C(=O)CCl)CCC2
HCID21491380

未命名化合物

结构：Sc1nc2cc(Cl)ccc2s1
HCID178527796

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cccc2c1N(C(=O)CSc1nc3cc(Cl)ccc3s1)CCC2
HCID59467883

未命名化合物

收率 56%

PROCEDURE

实验过程

The title compound was synthesized according to General Procedure A using compound 2 as the electrophile and 5-chloro-2-mercaptobenzothiazole as the nucleophile to yield 15 (3.60 g, 56%): MS m/z: 393 (M+H)+. Anal. Calcd. For, C19H17ClN2OS2.0.2H2O: C, 58.14; H, 4.47; N, 7.14; S, 16.33; Cl, 9.03. Found: C, 57.90; H, 4.40; N, 7.17; S, 16.47; Cl, 9.24.

WORKUP

后处理

  1. customThe title compound was synthesized