HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Methyl-1,2,3,4-tetrahydroquinoline → 2-(Benzo[d]thiazol-2-ylthio)-1-(6-methyl-3,4-dihydroquinolin-1(2H)-yl)ethanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Methyl-1,2,3,4-tetrahydroquinoline | HCID 66678 | — |
| Reactant | 2-(2-Benzothiazolylthio)acetic acid | HCID 80525 | — |
| Product | 2-(Benzo[d]thiazol-2-ylthio)-1-(6-methyl-3,4-dihydroquinolin-1(2H)-yl)ethanone | HCID 59467905 | 85% |
Reaction Steps
The title compound was synthesized according to General Procedure B using 2-(benzo[d]thiazol-2-ylthio)acetic acid and 6-methyl-1,2,3,4-tetrahydroquinoline to yield 38 (450.5 mg, 85%): MS (APCI): m/z 355 [M+H]+. Anal. Calcd. for C19H18N2OS2: C, 64.39; H, 5.12; N, 7.90. Found: C, 64.55; H, 5.01; N, 7.88.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08916550B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-08c6824ee8434ba38c242567e0e5966f |
| Source note | uspto-grants-2014_12 |