1,2,3,4-Tetrahydroquinoxaline → HCID 59467890, compound

HRID 1404929Notes

Reaction equation

HRID 1404929 reaction equation
[S:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=[C:2]1[S:10][CH2:11][C:12]([OH:14])=O.[NH:15]1[C:24]2[C:19](=[CH:20][CH:21]=[CH:22][CH:23]=2)[NH:18][CH2:17][CH2:16]1>>[S:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=[C:2]1[S:10][CH2:11][C:12]([N:15]1[C:24]2[C:19](=[CH:20][CH:21]=[CH:22][CH:23]=2)[NH:18][CH2:17][CH2:16]1)=[O:14]

Participants

3

Reactant 2

HCID 770281,2,3,4-TetrahydroquinoxalineHCID 805252-(2-Benzothiazolylthio)acetic acid

Product 1

HCID 59467890HCID 59467890, compoundYield 51%

Procedure

The title compound was synthesized according to General Procedure B using 2-(benzo[d]thiazol-2-ylthio)acetic acid and 1,2,3,4-tetrahydroquinoxaline to yield 41 as a white solid (51%) MS m/z: 342 (M+H)+. Anal. Calcd. For, C17H15N3OS2.0.2H2O: C, 59.18; H, 4.50; N, 12.18; S, 18.52. Found: C, 59.32; H, 4.65; N, 12.18; S, 18.25.

Workup

  1. customThe title compound was synthesized

Sources & evidence

ORD record
ord-79f719e8fcba4264825c2bc367f5612e
Source dataset
uspto-grants-2014_12
Patent number
US08916550B2

Reaction notes

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