HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylboronic Acid → 3-(4-Nitrophenyl)-4-phenylpyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylboronic Acid | HCID 66827 | — |
| Reactant | 4-Bromo-3-(4-nitrophenyl)pyridine | HCID 23246680 | — |
| Reactant | 4-(4-methylpyridin-3-yl)-1H-indazole | HCID 66715654 | — |
| Product | 3-(4-Nitrophenyl)-4-phenylpyridine | HCID 23246683 | — |
Reaction Steps
Intermediate 13B was prepared from Intermediate 13A and phenylboronic acid by the procedure described for the preparation of Intermediate 1C. The crude material was purified by silica gel chromatography (12 g ISCO column, eluting with 0 to 40% EtOAc in CH2Cl2) to yield Intermediate 13B. MS (ES): m/z=277.0 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08916553B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-2c5d95257dee404bbde5a466afba5ff7 |
| Source note | uspto-grants-2014_12 |