HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylpyridine-3-Boronic Acid → 3-(2-(2-Fluoroethoxy)-4-nitrophenyl)-4-methylpyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylpyridine-3-Boronic Acid | HCID 2762711 | — |
| Reactant | 4-(4-methylpyridin-3-yl)-1H-indazole | HCID 66715654 | — |
| Reactant | 1-Bromo-2-(2-fluoroethoxy)-4-nitrobenzene | HCID 86720061 | — |
| Product | 3-(2-(2-Fluoroethoxy)-4-nitrophenyl)-4-methylpyridine | HCID 86720062 | — |
Reaction Steps
Intermediate 16C was prepared from Intermediate 1A and Intermediate 16B by the procedure described for the preparation of Intermediate 1C, and was obtained as a beige solid (254 mg, 61% yield). MS (ES): m/z=277.0 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08916553B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-ec8d0d63f6a14eca92fc6575b0876260 |
| Source note | uspto-grants-2014_12 |