HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-chloro-N-{3-[(methylsulfonyl)methyl]phenyl}-1,3,5-triazin-2-amine → HCID 66576361, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-chloro-N-{3-[(methylsulfonyl)methyl]phenyl}-1,3,5-triazin-2-amine | HCID 21956343 | — |
| Reactant | 1403988-78-2 | HCID 53484320 | — |
| Product | HCID 66576361 | HCID 66576361 | — |
Reaction Steps
Example 15 was prepared under similar conditions as described in the preparation of Example 1 using crude 4-chloro-N-{3-[(methylsulfonyl)methyl]phenyl}-1,3,5-triazin-2-amine and 2-[2-(difluoromethoxy)-4-fluorophenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane (Focus Synthesis LLC). The batch was purified by preparative HPLC:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08916557B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-315111575a6347a784c594d6a49a02f1 |
| Source note | uspto-grants-2014_12 |