4-chloro-N-{3-[(methylsulfonyl)methyl]phenyl}-1,3,5-triazin-2-amine → HCID 66576592, compound

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Reaction Steps

Example 30 was prepared under similar conditions as described in the preparation of Example 1 using crude 4-chloro-N-{3-[(methylsulfonyl)methyl]phenyl}-1,3,5-triazin-2-amine and {5-fluoro-2-[(2-fluorobenzyl)oxy]phenyl}boronic acid (Combi-Blocks Inc.). The batch was purified by preparative TLC. 1H NMR (400 MHz, CDCl3, 300K) δ=8.84 (s, 1H), 7.79 (br, 1H), 7.63 (m, 2H), 7.48 (m, 2H), 7.37 (m, 1H), 7.27 (m, 1H), 7.09 (m, 5H), 5.22 (s, 2H), 4.23 (s, 2H), 2.78 (s, 3H).

Provenance & Evidence