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HRID1405194

反应详情

EQUATION

反应方程式

HRID 1405194 的结构方程式

REACTANTS

反应物

2
结构：CS(=O)(=O)Cc1cccc(Nc2ncnc(Cl)n2)c1
HCID21956343

未命名化合物

结构：OB(O)c1cc(F)ccc1OCc1cccc(F)c1
HCID43327941

{5-Fluoro-2-[(3-fluorophenyl)methoxy]phenyl}boronic acid

C13H11BF2O3

PRODUCTS

生成物

1
结构：CS(=O)(=O)Cc1cccc(Nc2ncnc(-c3cc(F)ccc3OCc3cccc(F)c3)n2)c1
HCID66576593

未命名化合物

PROCEDURE

实验过程

Example 31 was prepared under similar conditions as described in the preparation of Example 1 using crude 4-chloro-N-{3-[(methylsulfonyl)methyl]phenyl}-1,3,5-triazin-2-amine and {5-fluoro-2-[(3-fluorobenzyl)oxy]phenyl}boronic acid (Combi-Blocks Inc.). The batch was purified by preparative TLC (DCM/EtOH 95:5).

WORKUP

后处理

  1. customExample 31 was prepared under similar conditions
  2. customThe batch was purified by preparative TLC (DCM/EtOH 95:5)