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HRID1405195

反应详情

EQUATION

反应方程式

HRID 1405195 的结构方程式

REACTANTS

反应物

2
结构：COc1cc(Cl)ccc1B(O)O
HCID3858606

4-Chloro-2-methoxyphenylboronic acid

C7H8BClO3

结构：CS(=O)(=O)Cc1cccc(Nc2ncnc(Cl)n2)c1
HCID21956343

未命名化合物

PRODUCTS

生成物

1
结构：COc1cc(Cl)ccc1-c1ncnc(Nc2cccc(CS(C)(=O)=O)c2)n1
HCID66576594

未命名化合物

PROCEDURE

实验过程

Example 32 was prepared under similar conditions as described in the preparation of Example 30 using crude 4-chloro-N-{3-[(methylsulfonyl)methyl]phenyl}-1,3,5-triazin-2-amine and (4-chloro-2-methoxyphenyl)boronic acid (ABCR GmbH & CO. KG). The batch was purified by preparative HPLC.

WORKUP

后处理

  1. customExample 32 was prepared under similar conditions
  2. customThe batch was purified by preparative HPLC