Ethyl Acetate → HCID 70976465, compound

Participants

Reaction Steps

A solution of 1-(bromomethyl)-3-chloro-5-nitrobenzene (10.0 g) in ethanol (200 mL) was treated at −20° C. with portions of sodium methanthiolat (3.32 g) and stirred for 3 hours at room temperature. The reaction mixture was treated with brine (100 mL) extrakted with ethyl acetate (300 mL), washed with water (2×100 mL) and, dried with sodium sulfate and evaporated to dryness. One obtained the title compound (8.6 g) which was used without further purification.

Provenance & Evidence