N-Methylisatoic anhydride → HCID 71254516, compound

HRID 1405613Notes

Reaction equation

HRID 1405613 reaction equation
C[N:2]1[C:8](=O)[O:7][C:5](=O)[C:4]2=[CH:10][CH:11]=[CH:12][CH:13]=[C:3]12.[C:14]([NH:21][CH2:22][CH2:23][NH2:24])([O:16][C:17]([CH3:20])([CH3:19])[CH3:18])=[O:15]>>[C:17]([O:16][C:14](=[O:15])[NH:21][CH2:22][CH2:23][NH:24][C:5](=[O:7])[C:4]1[CH:10]=[CH:11][CH:12]=[CH:13][C:3]=1[NH:2][CH3:8])([CH3:20])([CH3:18])[CH3:19]

Participants

3

Reactant 2

HCID 25160N-Methylisatoic anhydrideHCID 187201N-BOC-ethylenediamine

Product 1

HCID 71254516HCID 71254516, compound

Procedure

Starting from N-methylisatoic anhydride and N-Boc-ethylenediamine and using Procedure S, the title compound was obtained as a slightly brown solid (903 mg; quantitative).

Sources & evidence

ORD record
ord-c9829fa16e0a4d8eb2bdc8656c951006
Source dataset
uspto-grants-2014_12
Patent number
US08916573B2

Reaction notes

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