HCID 47098616, compound → HCID 86660378, compound

HRID 1406441Notes

Reaction equation

HRID 1406441 reaction equation
[CH3:1][C:2]1[N:3]=[C:4]([NH:8][C:9](=[O:20])[C:10]2[CH:15]=[CH:14][C:13]([NH2:16])=[C:12]([N+:17]([O-])=O)[CH:11]=2)[S:5][C:6]=1[CH3:7]>[Ni].CO>[CH3:1][C:2]1[N:3]=[C:4]([NH:8][C:9](=[O:20])[C:10]2[CH:15]=[CH:14][C:13]([NH2:16])=[C:12]([NH2:17])[CH:11]=2)[S:5][C:6]=1[CH3:7]

Participants

4

Reactant 1

HCID 47098616HCID 47098616, compound

Product 1

HCID 86660378HCID 86660378, compound

Reagents, catalysts & solvents 2

HCID 935NickelCatalystHCID 887MethanolSolvent

Procedure

Prepared analogously to example 14b by hydrogenation of the product obtained in 77a using Raney nickel in methanol.

Workup

  1. customPrepared analogously to example 14b by hydrogenation of the product

Sources & evidence

ORD record
ord-5b5a078b68464148a26f90aab782bc64
Source dataset
uspto-grants-2014_12
Patent number
US08916599B2

Reaction notes

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