Thionyl Chloride → HCID 86660381, compound

HRID 1406472Notes

Reaction equation

HRID 1406472 reaction equation

[NH2:1][C:2]1[C:10]([N+:11]([O-:13])=[O:12])=[CH:9][C:5]([C:6](O)=[O:7])=[C:4]([CH3:14])[CH:3]=1.S(Cl)([Cl:17])=O>ClC(Cl)C>[NH2:1][C:2]1[C:10]([N+:11]([O-:13])=[O:12])=[CH:9][C:5]([C:6]([Cl:17])=[O:7])=[C:4]([CH3:14])[CH:3]=1

Participants

4

Reactant 2

HCID 24386Thionyl Chloride

HCID 45089373HCID 45089373, compound

Product 1

HCID 86660381HCID 86660381, compound

Reagents, catalysts & solvents 1

HCID 63651,1-DichloroethaneSolvent

Procedure

Prepared analogously to example 53a from 4-amino-2-methyl-5-nitro-benzoic acid and thionyl chloride in dichloroethane.

Sources & evidence

ORD record: ord-ea60580de8d845c58a583430cb1d5c3a
Source dataset: uspto-grants-2014_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08916599B2

Reaction notes

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