HCID 16003602, compound → HCID 67229883, compound

HRID 1406489Notes

Reaction equation

HRID 1406489 reaction equation
[CH2:1]([O:3][C:4](=[O:19])[C:5]1[CH:10]=[CH:9][C:8](NCCOC)=[C:7]([N+:16]([O-])=O)[CH:6]=1)[CH3:2]>C(O)C.[Pd]>[CH2:1]([O:3][C:4](=[O:19])[C:5]1[CH:10]=[CH:9][C:8]([CH2:2][CH2:1][O:3][CH3:4])=[C:7]([NH2:16])[CH:6]=1)[CH3:2]

Participants

4

Reactant 1

HCID 16003602HCID 16003602, compound

Product 1

HCID 67229883HCID 67229883, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 702EthanolSolvent

Procedure

Prepared analogously to example 1b by hydrogenation of 4-(2-methoxy-ethylamino)-3-nitro-benzoic acid ethyl ester using palladium/charcoal 10% in ethanol.

Sources & evidence

ORD record
ord-d81797f9471f433983e5dd1c9938b5d7
Source dataset
uspto-grants-2014_12
Patent number
US08916599B2

Reaction notes

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