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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1406495Generated: October 31, 2026

Dicyclohexylcarbodiimide → HCID 178524175, compound

https://huagongshe.com/reaction/1406495

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDicyclohexylcarbodiimideHCID 10868—
Reactant1,3-Dichloro-2-isothiocyanatobenzeneHCID 123239—
ReactantEthyl 3,4-DiaminobenzoateHCID 458855—
SolventEthanolHCID 702—
SolventDimethylformamideHCID 6228—
SolventSodium HydroxideHCID 14798—
ProductHCID 178524175HCID 178524175—

Reaction Steps

Prepared analogously to Example 113a from 3,4-diamino-benzoic acid ethyl ester and 1,3-dichloro-2-isothiocyanato-benzene with DCC in DMF and NaOH in ethanol.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08916599B2
Source datasetuspto-grants-2014_12
ORD IDord-9e7aef48939d42ac9a546d639183ff25
Source noteuspto-grants-2014_12