HCID 86660386, compound → HCID 67232818, compound

HRID 1406501Notes

Reaction equation

HRID 1406501 reaction equation
[N+:1]([C:4]1[CH:5]=[C:6]([CH:20]=[CH:21][C:22]=1[N+:23]([O-])=O)[C:7]([NH:9][C:10]1[CH:15]=[C:14]([C:16]([F:19])([F:18])[F:17])[CH:13]=[CH:12][N:11]=1)=[O:8])([O-])=O>CO.[Pd]>[NH2:1][C:4]1[CH:5]=[C:6]([CH:20]=[CH:21][C:22]=1[NH2:23])[C:7]([NH:9][C:10]1[CH:15]=[C:14]([C:16]([F:19])([F:17])[F:18])[CH:13]=[CH:12][N:11]=1)=[O:8]

Participants

4

Reactant 1

HCID 86660386HCID 86660386, compound

Product 1

HCID 67232818HCID 67232818, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 887MethanolSolvent

Procedure

Prepared analogously to example 1b by hydrogenation of 3,4-dinitro-N-(4-trifluoromethyl-pyridin-2-yl)-benzamide using palladium/charcoal 10% in methanol.

Sources & evidence

ORD record
ord-0652394abed54cb9880ad7419d8114ad
Source dataset
uspto-grants-2014_12
Patent number
US08916599B2

Reaction notes

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