1,3-Dichloro-2-isothiocyanatobenzene → HCID 86660399, compound

HRID 1406540Notes

Reaction equation

HRID 1406540 reaction equation
[CH2:1]([O:3][C:4](=[O:19])[C:5]1[CH:10]=[C:9]([NH2:11])[C:8]([NH2:12])=[CH:7][C:6]=1[O:13][CH2:14][C:15]([F:18])([F:17])[F:16])[CH3:2].[Cl:20][C:21]1[CH:26]=[CH:25][CH:24]=[C:23]([Cl:27])[C:22]=1[N:28]=[C:29]=[S:30]>C(#N)C>[NH2:12][C:8]1[C:9]([NH:11][C:29]([NH:28][C:22]2[C:23]([Cl:27])=[CH:24][CH:25]=[CH:26][C:21]=2[Cl:20])=[S:30])=[CH:10][C:5]([C:4]([O:3][CH2:1][CH3:2])=[O:19])=[C:6]([O:13][CH2:14][C:15]([F:16])([F:18])[F:17])[CH:7]=1

Participants

4

Reactant 2

HCID 1232391,3-Dichloro-2-isothiocyanatobenzeneHCID 67230020HCID 67230020, compound

Product 1

HCID 86660399HCID 86660399, compound

Reagents, catalysts & solvents 1

HCID 6342AcetonitrileSolvent

Procedure

Prepared analogously to example 583h from ethyl-4,5-diamino-2-(2,2,2-trifluoro-ethoxy)-benzoate (synthesis described at example 575) and 2,6-dichloro-1-isothiocyanato-benzene in acetonitrile.

Sources & evidence

ORD record
ord-a2743b051a8541a488075cd2cea53955
Source dataset
uspto-grants-2014_12
Patent number
US08916599B2

Reaction notes

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