HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Oxycodone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | (4R,4aS,12bS)-4a-hydroxy-9-methoxy-3-methyl-2,4,7a,13-tetrahydro-1H-4,12-methanobenzofuro[3,2-e]isoquinolin-7-one | HCID 5359420 | — |
| Reactant | Codeinone | HCID 5459910 | — |
| Product | Oxycodone | HCID 5284603 | — |
Reaction Steps
A blank 0.1 M HCl, 0.25 mg/mL standards of 14-hydroxycodeinone and codeinone, 0.58 μg/mL and 0.58 μg/mL of an oxycodol in 0.1M HCL standard were prepared and then analysed using the above method. ˜1 mg/mL samples of the post hydrogenation liquors and isolated oxycodone alkaloid were also prepared in 0.1M HCl.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08916707B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-d9513ed4fb174f6e98b9c59c4af3489f |
| Source note | uspto-grants-2014_12 |