HRID1407427

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID7249

3,4-Dimethylphenol

C8H10O

结构：O=C1C(=O)N(C(c2ccccc2)c2ccccc2)c2ccccc21

HCID1969277

1-(diphenylmethyl)-1H-indole-2,3-dione

C21H15NO2

HCID12236540

2,3-dihydrobenzofuran-6-ol

C8H8O2

结构：O=C1C(=O)N(C[C@H]2CCCO2)c2cc3c(cc21)OCCO3

HCID68598516

未命名化合物

PRODUCTS

生成物

结构：O=C1N(C[C@H]2CCCO2)c2cc3c(cc2C1(O)c1cc2c(cc1O)OCC2)OCCO3

HCID68598145

未命名化合物

PROCEDURE

实验过程

Following the procedure as described in PREPARATION 6A, and making non-critical variations using 2,3-dihydrobenzofuran-6-ol to replace 3,4-dimethylphenol, and 6-[(2R)-tetrahydrofuran-2-ylmethyl]-2,3-dihydro-6H-[1,4]dioxino[2,3-f]indole-7,8-dione to replace 1-(diphenylmethyl)-1H-indole-2,3-dione, 8-hydroxy-8-(6-hydroxy-2,3-dihydro-1-benzofuran-5-yl)-6-[(2R)-tetrahydrofuran-2-ylmethyl]-2,3,6,8-tetrahydro-7H-[1,4]dioxino[2,3-f]indol-7-one was obtained: Rf 0.45 (ethyl acetate/hexanes, 1/1); MS (ES+) m/z 408.1 (M−17).