化工社化工社 化学情報印刷レポート · 研究参考用
HCID 67358415、化合物 → HCID 68599194、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | HCID 67358415 | HCID 67358415 | — |
| 反応物 | 1-(diphenylmethyl)-3-hydroxy-3-(5-hydroxy-1-benzothiophen-6-yl)-1,3-dihydro-2H-indol-2-one | HCID 68598097 | — |
| 生成物 | HCID 68599194 | HCID 68599194 | — |
反応手順
Following the procedure as described in PREPARATION 82C and making non-critical variations using 1-(diphenylmethyl)-3-hydroxy-3-(5-hydroxy-1-benzothiophen-6-yl)-1,3-dihydro-2H-indol-2-one to replace 1-(diphenylmethyl)-4-fluoro-3-hydroxy-3-(7-hydroxy-2,3-dihydro-1,4-benzodioxin-6-yl)-1,3-dihydro-2H-indol-2-one, 1-(diphenylmethyl)-3-(5-hydroxy-1-benzothiophen-6-yl)-1,3-dihydro-2H-indol-2-one was obtained (94%) as an off-white solid: MS (ES+) m/z 448.1 (M+1).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08916580B2 |
| 出典データセット | uspto-grants-2014_12 |
| ORD ID | ord-79dd38a62e8a4795878e3999b32fe4fe |
| 出典メモ | uspto-grants-2014_12 |