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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1408265Generated: November 1, 2026

Methanol → HCID 178462738, compound

https://huagongshe.com/reaction/1408265

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanolHCID 887—
Reactant1-BromooctaneHCID 8140—
Reactant1-VinylimidazoleHCID 66171—
SolventDiethyl EtherHCID 3283—
ProductHCID 178462738HCID 178462738—

Reaction Conditions

Temperature60 °C

Reaction Steps

(From Yuan & Antonietti, DOI: 10.1021/ma102858b.) A solution/suspension comprising 0.1 mol of 1-vinylimidazole, 0.1 mol of n-octyl bromide and 30 mL of methanol were loaded into a 100 mL reactor. The mixture was stirred at 60° C. for 15 h. After cooling the reaction mixture was added dropwise into 1 L of diethyl ether. The precipitate was filtered off and dried at room temperature to yield a yellow liquid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08920682B2
Source datasetuspto-grants-2014_12
ORD IDord-532aa4eac3e042cda6e93cd569a32ba8
Source noteuspto-grants-2014_12