Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | 1-Bromohexadecane | HCID 8213 | — |
| Reactant | 1-Vinylimidazole | HCID 66171 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 178462742 | HCID 178462742 | — |
Reaction Steps
(From Yuan & Antonietti, DOI: 10.1021/ma102858b.) A solution/suspension comprising 0.1 mol of 1-vinylimidazole, 0.1 mol of n-hexadecyl bromide and 30 mL of methanol were loaded into a 100 mL reactor. The mixture was stirred at 60° C. for 15 h. After cooling the reaction mixture was added dropwise into 1 L of diethyl ether. The white precipitate was filtered off and dried at room temperature to yield a powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08920682B2 |
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| Source dataset | uspto-grants-2014_12 |
|---|
| ORD ID | ord-5c7f4e69bc544c21b5469f51fc346599 |
|---|
| Source note | uspto-grants-2014_12 |
|---|
