HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-4,6-bis(morpholin-4-yl)-1,3,5-triazine → HCID 58507827, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-4,6-bis(morpholin-4-yl)-1,3,5-triazine | HCID 224967 | — |
| Reactant | 3-(Tetramethyl-1,3,2-dioxaborolan-2-yl)benzonitrile | HCID 2760590 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 58507827 | HCID 58507827 | 57% |
Reaction Steps
Following the general procedure A, 4,4′-(6-chloro-1,3,5-triazine-2,4-diyl)dimorpholine was coupled with 3-cyanophenylboronic acid pinacol ester with reaction time of 15 h. Column chromatography (hexane/ethyl acetate 1:1) gave 57% of the title compound as an colorless solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08921361B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-663fbccc59ea4e929fead880ce853af2 |
| Source note | uspto-grants-2014_12 |