HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 58424408, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 4-(4-Bromophenoxy)butanoic acid | HCID 2384454 | — |
| Product | HCID 58424408 | HCID 58424408 | 67% |
Reaction Steps
4-(4-Bromophenoxy)butanoic acid (39 g, 25.6 mmol) was dissolved in SOCl2 (100 ml) mixture was heated to refluxed overnight. the mixture was concentrated in vacuo to give 4-(4-bromophenoxy)butanoyl chloride (27.6 g, 67%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08921359B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-42fd8a53005d49de871f14990f2f29aa |
| Source note | uspto-grants-2014_12 |