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HRID1408995

反应详情

EQUATION

反应方程式

HRID 1408995 的结构方程式

REACTANTS

反应物

1
反应SMILES：Cl.Cl.N#Cc1ccc2[nH]cc(CCCCN3CCN(c4ccc5oc(C(N)=O)cc5c4)CC3)c2c1
HCID67300892

未命名化合物

PRODUCTS

产物

1
反应SMILES：Cl.N#Cc1ccc2[nH]cc(CCCCN3CCN(c4ccc5oc(C(N)=O)cc5c4)CC3)c2c1
HCID6918313

5-{4-[4-(5-Cyano-1H-indol-3-yl)butyl]piperazin-1-yl}-1-benzofuran-2-carboximidic acid--hydrogen chloride (1/1)

C26H28ClN5O2

AUXILIARIES

试剂、催化剂与溶剂

1
反应SMILES：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

10 g of 1-[4-(5-cyanoindol-3-yl)butyl]-4-(2-carbamoyl-benzofuran-5-yl)-piperazine dihydrochloride Form XIII are dispersed in 11 water. After stirring for 48 hours the crystals are recovered by filtration, and drying in vacuo to constant weight at room temperature leads to 1-[4-(5-cyanoindol-3-yl)butyl]-4-(2-carbamoyl-benzofuran-5-yl)-piperazine hydrochloride hydrate of Form V.

WORKUP

后处理

  1. filtrationare recovered by filtration
  2. customdrying in vacuo to constant weight at room temperature