HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 136377079, compound → HCID 178522818, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 136377079 | HCID 136377079 | — |
| Reactant | HCID 178499080 | HCID 178499080 | — |
| Product | HCID 178522818 | HCID 178522818 | — |
Reaction Steps
5,6-Dihydroxy-2-(1-phenyl-cyclopentylmethyl)-pyrimidine-4-carboxylic acid benzylamide was synthesized as an off-white solid (20 mg, 30%) from 55 mg of 5,6-dihydroxy-2-(1-phenyl-cyclopentylmethyl)-pyrimidine-4-carboxylic acid methyl ester following the procedure described for 5-hydroxy-6-oxo-2-(1-phenyl-cyclopentylmethyl)-1,6-dihydro-pyrimidine-4-carboxylic acid methylamide (Example 9). LCMS: m/z=403.8 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08921388B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-c1ce55c9302d4bf0b2cc8245d223c379 |
| Source note | uspto-grants-2014_12 |