HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyrrolidine → HCID 136377085, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | HCID 136377081 | HCID 136377081 | — |
| Product | HCID 136377085 | HCID 136377085 | 54% |
Reaction Steps
The synthesis was performed as in Example 21 using methyl 2-(biphenyl-2-ylmethyl)-5-hydroxy-6-oxo-1,6-dihydropyrimidine-4-carboxylate (0.10 g, 298 μmol) and pyrrolidine (0.5 ml; 6.06 mmol) to provide the title compound as an off-white solid (0.059 g; 54%). LCMS: m/z=412 (MH+). LCMS: m/z=375 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08921388B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-19f7706a5e764f5ba126c00424ec5cf6 |
| Source note | uspto-grants-2014_12 |